GUO Chao-fei,HAO Jian-min,CHEN Yong-nan,CHEN Hong,DING Ye-li.Effect of Voltage on Growth Characteristics of Ceramic Coating Containing ZrO2 Prepared by Microarc Oxidation on TiAl Alloy[J],46(5):1-5
Effect of Voltage on Growth Characteristics of Ceramic Coating Containing ZrO2 Prepared by Microarc Oxidation on TiAl Alloy
Received:October 11, 2016  Revised:May 20, 2017
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DOI:10.16490/j.cnki.issn.1001-3660.2017.05.001
KeyWord:TiAl alloy  micro-arc oxidation  growth characteristics  ZrO2  coating thickness  voltage
              
AuthorInstitution
GUO Chao-fei School of Materials Science and Engineering, Chang'an University, Xi'an , China
HAO Jian-min School of Materials Science and Engineering, Chang'an University, Xi'an , China
CHEN Yong-nan School of Materials Science and Engineering, Chang'an University, Xi'an , China
CHEN Hong School of Materials Science and Engineering, Chang'an University, Xi'an , China
DING Ye-li Shandong Jiaotong University Maritime College, Weihai , China
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Abstract:
      The work aims to fabricate microarc oxide coating containing ZrO2 phase on TiAl alloy, and study effects of voltage on growth characteristics of microarc oxide coating. TiAl alloy samples were treated in soluble zirconate electrolyte at 480, 500 and 520 V, respectively. Eddy current thickness tester, SEM and XRD were used to observe thickness, microstructure and phase composition of the coating. Thickness of the coating prepared at 480, 500, 520 V was 18, 28, 48 μm, respectively. A small-scale increase in voltage caused a significant increase in coating thickness. Crystal phases of the coating were t-ZrO2 (primary), m-ZrO2, Al2O3, and TiO2. The content of m-ZrO2 increased slightly with the increase of voltage. Micropores and some ceramic particles of varying sizes were observed on coating surface. The pore diameter and coating roughness increased with the increase of voltage. The voltage has minor effect on phase composition of the coating and a significant impact on morphology. High voltage improves coating thickness, roughness and micropore diameter.
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