张继平,王鹏,郝利峰,戴媛静,李小磊.含磷极压抗磨剂抗微点蚀性能评价和机理分析[J].表面技术,2020,49(9):45-52.
ZHANG Ji-ping,WANG Peng,HAO Li-feng,DAI Yuan-jing,LI Xiao-lei.The Study of the Anti-micro-pitting Performance of the EP&AW Additives[J].Surface Technology,2020,49(9):45-52 |
| 含磷极压抗磨剂抗微点蚀性能评价和机理分析 |
| The Study of the Anti-micro-pitting Performance of the EP&AW Additives |
| 投稿时间：2020-07-13 修订日期：2020-09-20 |
| DOI：10.16490/j.cnki.issn.1001-3660.2020.09.004 |
| 中文关键词: 含磷极压抗磨剂 抗微点蚀 抗磨减摩 油膜厚度 摩擦氧化 抗腐蚀 |
| 英文关键词:EP&AW additive containing phosphorus anti-micro-pitting anti-wear & anti-friction oil film thickness friction oxidation anti-corrosion |
| 基金项目: |
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| Author | Institution |
| ZHANG Ji-ping | 1.Tianjin Research Institute for Advanced Equipment, Tsinghua University, Tianjin 300300, China |
| WANG Peng | 2.PetroChina Lanzhou Lubricating Oil R&D Institute, Lanzhou 730060, China |
| HAO Li-feng | 3.Qiuzhen College, Huzhou University, Huzhou 313000, China |
| DAI Yuan-jing | 4.Tsinghua University, Beijing 100084, China |
| LI Xiao-lei | 1.Tianjin Research Institute for Advanced Equipment, Tsinghua University, Tianjin 300300, China |
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| 中文摘要: |
| 目的 评价三种含磷极压抗磨剂的抗微点性能并分析其作用机理。方法 使用MPR模拟微点蚀试验机考察三种含磷极压抗磨剂（磷型P-1、硫磷型P-2、分散型P-3）的抗微点蚀性能。使用四球试验机、铜片腐蚀试验仪、烘箱、油膜厚度测试仪等，评价添加剂的摩擦、抗腐蚀、抗氧化性能及油膜形成能力，分析添加剂抗微点蚀性能与上述性能之间的关系。借助SEM测试分析不同添加剂的抗微点蚀机理。结果 添加P-3的润滑油GO-3的综合性能最好，GO-3具有良好的抗微点蚀性能，9 h MPR试验的辊子轨道宽度变化率为35.87%。GO-3具有良好的极压抗磨减摩性能，四球机试验测得其最大无卡咬负荷为1441.6 N，磨斑直径为0.38 mm，在试验载荷大于294 N时，其摩擦系数最低。GO-3的抗腐蚀性能良好，铜片腐蚀试验级别为1b。GO-3的氧化腐蚀性低，烘箱氧化试验中钢片评分为1分，且无油泥产生。GO-3的油膜形成能力强，60~120 ℃时弹性流体润滑油膜的厚度为371.2~153.6 nm。结论 分散型磷氮极压抗磨剂P-3化学活性适中，可以避免在摩擦表面发生严重腐蚀或剧烈摩擦化学反应，具有良好的承载、减摩、抗磨和抗微点蚀性能。 |
| 英文摘要: |
| To evaluate the anti-micro-pitting performances of three extreme pressure & antiwear (EP&AW) additives containing phosphorus, MPR tests which can simulate the micro-pitting conditions were conducted. Meanwhile, four-ball tribometer, copper corrosion tester, baking oven and lubricating film thickness meter were used to study the other performances of tribology, anti-corrosion, antioxidant and lubricating film. Moreover, mechanism of anti-micro-pitting was investigated in detail. The oil with dispersed phosphorus and nitrogen EP&AW additive can show the best overall performance. After 9 hours MPR test of the oil added with dispersed phosphorus and nitrogen EP&AW additive, change rate of MPR roll track width is 35.87%. With four-ball tribometer test of this oil, maximum non-seizure load of 1441.6 N is obtained, and its relevant wear diameter of ball is 0.38 mm. When test load of four-ball test is bigger than 294 N, friction coefficient of the oil with dispersed phosphorus and nitrogen EP&AW additive is the smallest. Moreover, anticorrosion and antioxidant performance of this oil is good, copper corrosion grade is 1b, and steel disc grade is 1 score with no oil sludge. The oil with dispersed phosphorus and nitrogen EP&AW additive can form lubricating film with thickness of 371.2~153.6 nm when temperature is 60~120 ℃. The dispersed phosphorus and nitrogen EP&AW additive possesses moderate chemical activity and shows the best overall performances. |
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