宿辉,王桂芳,栾风虎,胡胜鹏.(SiC)p表面低成本化学改性的研究[J].表面技术,2007,36(2):21-23. XU Hui,WANG Gui fang,LUAN Feng-hu,HU Sheng-peng.Study on Low Cost Chemistry Modification on ( SiC) p[J].Surface Technology,2007,36(2):21-23 |
(SiC)p表面低成本化学改性的研究 |
Study on Low Cost Chemistry Modification on ( SiC) p |
投稿时间:2006-10-27 修订日期:2007-04-10 |
DOI: |
中文关键词: ( SiC), 碳化硅复合粉体 表面改性 化学镀 热处理 |
英文关键词:( SiC)p ( Ni/SiC)p Surface modification Electroless plating Heat treatment |
基金项目:黑龙江省科技攻关项目( GC06A208);学院优秀青年基金( Q06002);黑龙江省自然科学基金(E2004-20) |
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Author | Institution |
XU Hui | Department of Materials and Chemistry Engineering, Heilongjiang Engineering Institute, Harbin 150050, China |
WANG Gui fang | Department of Materials Science and Engineering, Harbin Engineering University, Harbin 150001 , China |
LUAN Feng-hu | Department of Materials Science and Engineering, Harbin Engineering University, Harbin 150001 , China |
HU Sheng-peng | Department of Materials and Chemistry Engineering, Heilongjiang Engineering Institute, Harbin 150050, China |
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中文摘要: |
为解决裸(SiC)p在应用中存在的不足,提出(SiC)p表面低成本化学改性的思路。采用简单的化学镀技术,改进氧化、亲水、敏化和活化的前处理工艺,对(SiC)p进行表面化学改性。确定了最佳的试验工艺,获得了镀层连续、无光滑(SiC)p裸露的较高质量的碳化硅复合粉体[简写为( Ni/SiC)p],通过SEM、EDS、XRD、TEM等测试,结果表明:改性后的(Ni/SiC),较改性前的(SiC)p导电性有所提高,形貌、组成发生改变。同时分析了热处理对(Ni/SiC),的影响,结果表明:随着温度的升高,(Ni/SiC),表面改性层中的镍由非晶态转化为晶态。 |
英文摘要: |
For solving shortage of naked ( SiC)p in the application, the surface low cost chemistry modification on ( SiC) p was expound. The simple electroless plating improved the pre-treatments technology including oxidation, ge- ting close to water, sensitization and activation process. The continual, non-lubricous and high quality decoration of ( SiC)p( abbreviate as ( Ni/SiC)p) was obtained. Experiment results of SEM, EDS, XRD and TEM indicate that the e- lectric functions of ( Ni/SiC) p is much higher than those of unembellished ( SiC)p, and morphology and structure of ( Ni/SiC)p are changed. The effect of heat treatment on ( Ni/SiC)p was also analyzed. The result expresses that along with the temperature, the non-crystalline state nickel in surface modified layer on ( Ni/SiC) p becomes crystalline state nickel along with the going up of temperature. |
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